{"id":87307,"date":"2023-07-20T14:14:14","date_gmt":"2023-07-20T06:14:14","guid":{"rendered":"http:\/\/www.broadbio.com\/?p=87307"},"modified":"2023-07-20T14:14:19","modified_gmt":"2023-07-20T06:14:19","slug":"%e5%8a%a0%e6%8b%bf%e5%a4%a7nrc%e6%a0%87%e5%87%86%e5%93%81gonyautoxins-5%e7%9a%84%e8%ae%a4%e8%af%81%e6%a0%a1%e5%87%86%e6%ba%b6%e6%b6%b2%e8%ae%a1%e9%87%8f%e6%ba%af%e6%ba%90","status":"publish","type":"post","link":"http:\/\/www.broadbio.com\/archives\/87307","title":{"rendered":"\u52a0\u62ff\u5927NRC\u6807\u51c6\u54c1Gonyautoxins-5\u7684\u8ba4\u8bc1\u6821\u51c6\u6eb6\u6db2\u8ba1\u91cf\u6eaf\u6e90"},"content":{"rendered":"\n

Certified Calibration Solution for Gonyautoxin-5\/ Gonyautoxin-5\u7684\u8ba4\u8bc1\u6821\u51c6\u6eb6\u6db2<\/p>\n\n\n\n

Gonyautoxin-5 (GTX5)<\/strong><\/p>\n\n\n\n

CAS registry No.: 64296-25-9 (free base)<\/p>\n\n\n\n

InChIKey: JKKCSFJSULZNDN-HGRQIUPRSA-N (free base)<\/p>\n\n\n\n

Molecular formula: C10H17N7O7S1 <\/p>\n\n\n\n

Molecular weight: 379.35 g\/mol<\/p>\n\n\n\n

CRM-GTX5-d<\/strong>\u7684\u5236\u5907<\/strong><\/p>\n\n\n\n

N-\u78fa\u57fa\u6c28\u57fa\u7532\u9170\u57fa-\u739b\u7459\u6bd2\u7d20-3\uff08C2\uff09\u662f\u4ece\u4e9a\u5386\u5c71\u5927\u85fb\u7684\u5927\u89c4\u6a21\u5b9e\u9a8c\u5ba4\u57f9\u517b\u7269\u4e2d\u5206\u79bb\u51fa\u6765\u7684\uff0c\u5316\u5b66\u8f6c\u5316\u4e3aGTX5\uff0c\u7136\u540e\u901a\u8fc7\u51e0\u4e2a\u8272\u8c31\u6b65\u9aa4\u7eaf\u5316[4]\u3002GTX5\u7684\u7ed3\u6784\u548c\u7eaf\u5ea6\u901a\u8fc7LC-MS\/MS[5\uff0c6]\uff08\u56fe1\u548c\u56fe2\uff09\u548c1H NMR\u8fdb\u884c\u4e86\u786e\u8ba4\u3002\u5bf9\u4e8eGTX5\uff08\u6e38\u79bb\u78b1\uff09\u7684[m+H]+\u79bb\u5b50\uff0c\u4f7f\u7528LC\u9ad8\u5206\u8fa8\u7387MS\uff08LC-HRMS\uff09\u83b7\u5f97\u4e86380.0984\u7684\u6d4b\u91cf\u51c6\u786em\/z\uff08\u5bf9\u4e8eC10H18N7O S+\uff0c\u2206=0.2 ppm\uff09\u3002\u901a\u8fc7LC-MS\u3001LC-ox-FLD[7]\uff08\u56fe3\uff09\u3001\u7d2b\u5916\u6bdb\u7ec6\u7ba1\u7535\u6cf3\uff08CE-UV\uff09[8]\u548c\u5316\u5b66\u53d1\u5149\u6c2e\u68c0\u6d4b\u6db2\u76f8\u8272\u8c31\u6cd5\uff08LC-CLND\uff09[9]\u8fdb\u4e00\u6b65\u8bc4\u4f30\u7eaf\u5ea6\u3002<\/p>\n\n\n\n

\u52a0\u62ff\u5927NRC\u6807\u51c6\u54c1Gonyautoxins-5\u7684\u8ba4\u8bc1\u6821\u51c6\u6eb6\u6db2<\/strong>\u901a\u8fc7\u5728H2O\u4e2d\u7a00\u91ca\u7eaf\u5316\u7684GTX5\u4ee5\u4f7f\u75281H-NMR\uff08qNMR\uff09\u8fdb\u884c\u5b9a\u91cf\u6765\u5236\u5907\u50a8\u5907\u6eb6\u6db2[10]\u3002CRM-GTX5-d\u6eb6\u6db2\u662f\u901a\u8fc7\u5728\u7528\u4e59\u9178\u8c03\u8282\u81f3pH 5\u7684\u8131\u6c14\u53bb\u79bb\u5b50\u6c34\u4e2d\u5bf9\u50a8\u5907\u6eb6\u6db2\u8fdb\u884c\u7cbe\u786e\u7a00\u91ca\u800c\u5236\u5907\u7684\u3002\u5c06\u7b49\u5206\u8bd5\u6837\u5206\u914d\u5230\u5145\u6ee1\u6c29\u6c14\u7684\u7425\u73c0\u8272\u73bb\u7483\u5b89\u74ff\u4e2d\uff0c\u5e76\u7acb\u5373\u8fdb\u884c\u706b\u7130\u5bc6\u5c01\u3002\u6bcf\u4e2a\u5b89\u74ff\u542b\u6709\u5927\u7ea60.5\u6beb\u5347\u6eb6\u6db2\u3002<\/p>\n\n\n\n

\u540c\u8d28\u6027<\/p>\n\n\n\n

\u52a0\u62ff\u5927NRC\u6807\u51c6\u54c1Gonyautoxins-5\u7684\u8ba4\u8bc1\u6821\u51c6\u6eb6\u6db2<\/strong>\u4ece\u6574\u4e2a\u704c\u88c5\u7cfb\u5217\u4e2d\u9009\u62e9\u4ee3\u8868\u6027\u6570\u91cf\u7684CRM-GTX5-d\u5b89\u74ff\uff0c\u5e76\u901a\u8fc7LC-ox-FLD\u6d4b\u91cfGTX5\u54cd\u5e94\u3002\u672a\u89c2\u5bdf\u5230\u5f02\u8d28\u6027\u3002<\/p>\n\n\n\n

\u7a33\u5b9a\u6027<\/strong><\/p>\n\n\n\n

\u52a0\u62ff\u5927NRC\u6807\u51c6\u54c1Gonyautoxins-5\u7684\u8ba4\u8bc1\u6821\u51c6\u6eb6\u6db2<\/strong>\u5bf9CRM-GTX5-c\u8fdb\u884c\u7684\u4e00\u5e74\u7a33\u5b9a\u6027\u7814\u7a76\u8868\u660e\uff0cGTX5\u5728-12\u00b0c\u6216\u66f4\u4f4e\u6e29\u5ea6\u4e0b\u50a8\u5b58\u5728\u5bc6\u5c01\u5b89\u74ff\u4e2d\u7684\u4e59\u9178\u6c34\u6eb6\u6db2\uff08pH 5\uff09\u4e2d\u5177\u6709\u826f\u597d\u7684\u7a33\u5b9a\u6027\u3002<\/p>\n\n\n\n

\u5b89\u5168\u8bf4\u660e<\/strong><\/p>\n\n\n\n

\u52a0\u62ff\u5927NRC\u6807\u51c6\u54c1Gonyautoxins-5\u7684\u8ba4\u8bc1\u6821\u51c6\u6eb6\u6db2<\/strong>\u5982\u679c\u6444\u5165\u8db3\u591f\u7684\u91cf\uff0cGTX5\u548c\u76f8\u5173\u6bd2\u7d20\u53ef\u80fd\u5bfc\u81f4\u762b\u75ea\u751a\u81f3\u6b7b\u4ea1\u3002\u53ea\u6709\u5408\u683c\u7684\u4eba\u5458\u624d\u80fd\u5904\u7406\u6eb6\u6db2\uff0c\u5e76\u5e94\u4f7f\u7528\u9002\u5f53\u7684\u5904\u7406\u65b9\u6cd5\u3002\u5728\u73bb\u7483\u7834\u788e\u7684\u60c5\u51b5\u4e0b\u6253\u5f00\u5b89\u74ff\u65f6\uff0c\u5e94\u4f7f\u7528\u5408\u9002\u7684\u4e2a\u4eba\u9632\u62a4\u8bbe\u5907\u3002CRM-GTX5-d\u63d0\u4f9b\u4e86\u5b89\u5168\u6570\u636e\u8868\uff08SDS\uff09\u3002<\/p>\n\n\n\n

\u6709\u6548\u671f<\/strong><\/p>\n\n\n\n

\u52a0\u62ff\u5927NRC\u6807\u51c6\u54c1Gonyautoxins-5\u7684\u8ba4\u8bc1\u6821\u51c6\u6eb6\u6db2<\/strong>\u5982\u679c\u5728\u5efa\u8bae\u7684-12\u00b0C\u6216\u66f4\u4f4e\u7684\u50a8\u5b58\u6761\u4ef6\u4e0b\u672a\u5f00\u5c01\u50a8\u5b58\uff0c\u5219CRM-GTX5-d\u7684\u8ba4\u8bc1\u6d53\u5ea6\u6709\u6548\u671f\u4e3a\u81ea\u9500\u552e\u4e4b\u65e5\u8d771\u5e74\u3002<\/p>\n\n\n\n

\u8ba1\u91cf\u6eaf\u6e90\u6027<\/strong><\/p>\n\n\n\n

\u672c\u8bc1\u4e66\u4e2d\u63d0\u4f9b\u7684\u7ed3\u679c\u53ef\u8ffd\u6eaf\u5230SI\uff08Syst\u00e8me\ninternational d\u2019unit\u00e9s\uff09\uff0c\u901a\u8fc7NIST\u90bb\u82ef\u4e8c\u7532\u9178\u6c22\u94be\u8ba4\u8bc1\u53c2\u8003\u6750\u6599\uff08NIST SRM 84L\uff09\u548cGTX5\uff08NRC CRM-GTX5-c\uff09\u8ba4\u8bc1\u53c2\u8003\u6750\u6599\u7684\u91cd\u91cf\u5236\u5907\u6807\u51c6\u3002<\/p>\n","protected":false},"excerpt":{"rendered":"

Certified Calibration Solution for Gonyautoxin-5\/ Gonya […]<\/p>\n","protected":false},"author":2,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","theme-transparent-header-meta":"","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"ast-content-background-meta":{"desktop":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"footnotes":""},"categories":[92],"tags":[],"_links":{"self":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/posts\/87307"}],"collection":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/users\/2"}],"replies":[{"embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/comments?post=87307"}],"version-history":[{"count":1,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/posts\/87307\/revisions"}],"predecessor-version":[{"id":87314,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/posts\/87307\/revisions\/87314"}],"wp:attachment":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/media?parent=87307"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/categories?post=87307"},{"taxonomy":"post_tag","embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/tags?post=87307"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}