{"id":104259,"date":"2025-09-16T09:29:41","date_gmt":"2025-09-16T01:29:41","guid":{"rendered":"http:\/\/www.broadbio.com\/?post_type=product&#038;p=104259"},"modified":"2025-09-16T09:29:50","modified_gmt":"2025-09-16T01:29:50","slug":"nist-srm-1957%e5%86%bb%e5%b9%b2%e9%9d%9e%e5%bc%ba%e5%8c%96%e4%ba%ba%e4%bd%93%e8%a1%80%e6%b8%85%e4%b8%ad%e7%9a%84%e6%9c%89%e6%9c%ba%e6%b1%a1%e6%9f%93%e7%89%a9%e6%a0%87%e5%87%86%e5%93%81","status":"publish","type":"product","link":"http:\/\/www.broadbio.com\/product\/nist-srm-1957%e5%86%bb%e5%b9%b2%e9%9d%9e%e5%bc%ba%e5%8c%96%e4%ba%ba%e4%bd%93%e8%a1%80%e6%b8%85%e4%b8%ad%e7%9a%84%e6%9c%89%e6%9c%ba%e6%b1%a1%e6%9f%93%e7%89%a9%e6%a0%87%e5%87%86%e5%93%81","title":{"rendered":"NIST SRM 1957\u51bb\u5e72\u975e\u5f3a\u5316\u4eba\u4f53\u8840\u6e05\u4e2d\u7684\u6709\u673a\u6c61\u67d3\u7269\u6807\u51c6\u54c1"},"content":{"rendered":"<table>\n<tbody>\n<tr>\n<td width=\"156\">\u4ea7\u54c1\u8d27\u53f7<\/td>\n<td width=\"569\"><strong>SRM 1957\/NIST SRM 1957<\/strong><\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u4ea7\u54c1\u540d\u79f0<\/td>\n<td width=\"569\"><strong>Organic Contaminants in Non-Fortified Human Serum<\/strong><\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u4e2d\u6587\u540d\u79f0<\/td>\n<td width=\"569\"><strong>\u975e\u5f3a\u5316\u4eba\u4f53\u8840\u6e05\u4e2d\u7684\u6709\u673a\u6c61\u67d3\u7269\u6807\u51c6\u53c2\u8003\u7269\u8d28<\/strong><strong>\/<\/strong><strong>\u4eba\u8840\u6e05\u4e2d\u7684\u591a\u6c2f\u8054\u82ef\uff08<\/strong><strong>PCB<\/strong><strong>\uff09\u540c\u7cfb\u7269\u3001\u6c2f\u5316\u519c\u836f\u548c\u591a\u6eb4\u4e8c\u82ef\u919a\uff08<\/strong><strong>PBDE<\/strong><strong>\uff09\u540c\u7cfb\u7269<\/strong><strong>\u6807\u51c6\u7269\u8d28\/<\/strong><strong>\u51bb\u5e72\u975e\u5f3a\u5316\u4eba\u4f53\u8840\u6e05\u4e2d\u7684\u6709\u673a\u6c61\u67d3\u7269\u6807\u51c6\u54c1<\/strong><\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u4ea7\u54c1\u89c4\u683c<\/td>\n<td width=\"569\">5 vials<\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u4ea7\u54c1\u8be6\u60c5<\/td>\n<td width=\"569\">\u7528\u4e8e\u8bc4\u4f30\u6d4b\u5b9a\u4eba\u4f53\u8840\u6e05\u548c\u7c7b\u4f3c\u57fa\u8d28\u4e2d\u9009\u5b9a\u7684\u591a\u6c2f\u8054\u82ef\uff08PCB\uff09\u540c\u7cfb\u7269\u3001\u6c2f\u5316\u519c\u836f\u548c\u591a\u6eb4\u4e8c\u82ef\u919a\uff08PBDE\uff09\u540c\u7cfb\u7269\u7684\u5206\u6790\u65b9\u6cd5\u3002\u63d0\u4f9b\u4e86\u9009\u5b9a\u7684\u591a\u6c2f\u4e8c\u82ef\u5e76\u5bf9\u4e8c\u6076\u82f1\uff08PCDDs\uff09\u3001\u591a\u6c2f\u4e8c\u5e76\u544b\u5583\uff08PCDFs\uff09\u3001\u5168\u6c1f\u5316\u5408\u7269\uff08PFCs\uff09\u548c\u8840\u8102\u7684\u53c2\u8003\u503c\u3002\u63d0\u4f9b\u4e86\u6240\u9009\u7f9f\u57fa\u5316\u5316\u5408\u7269\u7684\u4fe1\u606f\u503c\u3002<\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u4ea7\u54c1\u6709\u6548\u671f<\/td>\n<td width=\"569\">31-Aug-25<\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u8bc1\u4e66\u66f4\u65b0\u65f6\u95f4<\/td>\n<td width=\"569\">26-Jan-16<\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u50a8\u5b58\u6e29\u5ea6<\/td>\n<td width=\"569\">\u51b7\u85cf4\u6444\u6c0f\u5ea6\/\u6709\u5173\u6b64\u6750\u6599\u7684\u5b58\u50a8\u4fe1\u606f\uff0c\u8bf7\u53c2\u9605\u8bc1\u4e66\u3002<\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u5371\u9669\u7b49\u7ea7<\/td>\n<td width=\"569\">\u975e\u5371<\/td>\n<\/tr>\n<tr>\n<td width=\"156\">\u6613\u8150\u7c7b\u578b<\/td>\n<td width=\"569\">\u8fd9\u79cd\u6750\u6599\u6613\u8150\u70c2\uff0c\u7528\u51b7\u5305\u88c5\u8fd0\u8f93\u3002<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p><strong>NIST SRM 1957\u7a33\u5b9a\u6027\u548c\u50a8\u5b58\uff1a<\/strong>\u8840\u6e05\u7ecf\u8fc7\u51b7\u51bb\u5e72\u71e5\uff0c\u5e94\u57282\u00b0C\u81f38\u00b0C\u7684\u51b0\u7bb1\u4e2d\u50a8\u5b58\uff0c\u76f4\u81f3\u53ef\u4f9b\u4f7f\u7528\u3002\u5b83\u4e0d\u5e94\u88ab\u51b7\u51bb\u6216\u66b4\u9732\u5728\u9633\u5149\u6216\u7d2b\u5916\u7ebf\u8f90\u5c04\u4e0b\u3002\u91cd\u5efa\u540e\uff0c\u5e94\u7acb\u5373\u4f7f\u7528\u5185\u5bb9\u7269\uff0c\u6216\u5c06\u5176\u50a8\u5b58\u57282\u00b0C\u81f38\u00b0C\u4e4b\u95f4\uff0c\u76f4\u5230\u53ef\u4ee5\u4f7f\u7528\u4e3a\u6b62\uff0c\u6700\u597d\u57284\u5c0f\u65f6\u5185\u3002\u4e0d\u5efa\u8bae\u51b7\u51bb\u91cd\u5efa\u6750\u6599\u3002<\/p>\n<p><strong>\u4f7f\u7528\uff1a<\/strong>\u5c06\u5c0f\u74f6\u5347\u81f3\u5ba4\u6e29\uff0c\u53d6\u4e0b\u91d1\u5c5e\u76d6\uff0c\u8f7b\u8f7b\u62cd\u6253\u5c0f\u74f6\u5e95\u90e8\uff0c\u5c06\u4efb\u4f55\u5e72\u71e5\u7684\u8840\u6e05\u9897\u7c92\u4ece\u585e\u5b50\u4e2d\u53d6\u51fa\u3002\u5c0f\u5fc3\u5730\u53d6\u4e0b\u585e\u5b50\uff0c\u4ee5\u907f\u514d\u8840\u6e05\u9897\u7c92\u53ef\u80fd\u4e22\u5931\u3002\u4f7f\u7528\u5df2\u77e5\u7cbe\u5ea6\u7684\u5206\u914d\u5668\u572820\u00b0C\u81f325\u00b0C\u7684\u6e29\u5ea6\u4e0b\u7f13\u6162\u5411\u5c0f\u74f6\u4fa7\u9762\u6dfb\u52a010.7 mL\u84b8\u998f\u6c34\u6216HPLC\u7ea7\u6c34\uff0c\u540c\u65f6\u4e0d\u65ad\u8f6c\u52a8\u5c0f\u74f6\u3002\u66f4\u6362\u585e\u5b50\uff0c\u5c06\u5c0f\u74f6\u65cb\u8f6c\u4e24\u5230\u4e09\u6b21\uff0c\u9759\u7f6e\u7ea610\u5206\u949f\u3002\u901a\u8fc7\u8f7b\u8f7b\u65cb\u8f6c\u6df7\u5408\u5185\u5bb9\u7269\uff0c\u9759\u7f6e\u5927\u7ea630\u5206\u949f\uff0c\u518d\u6b21\u65cb\u8f6c\uff0c\u9759\u7f6e10\u5206\u949f\uff0c\u6700\u540e\u5c06\u5c0f\u74f6\u5012\u7f6e\u51e0\u6b21\u3002\u4e0d\u8981\u7528\u529b\u6447\u6643\uff0c\u5426\u5219\u4f1a\u4ea7\u751f\u6ce1\u6cab\u3002\u91cd\u5efa\u7684\u603b\u65f6\u95f4\u7ea6\u4e3a1\u5c0f\u65f6\u3002\u91cd\u5efa\u540e\uff0c\u5c3d\u5feb\u4f7f\u7528\u5185\u5bb9\u7269\uff0c\u6216\u57282\u00b0C\u81f38\u00b0C\u4e4b\u95f4\u50a8\u5b58\uff0c\u76f4\u5230\u5206\u6790\uff0c\u6700\u597d\u57284\u5c0f\u65f6\u5185\u3002<\/p>\n<p><strong>\u975e\u5f3a\u5316\u4eba\u4f53\u8840\u6e05\u4e2d\u7684\u6709\u673a\u6c61\u67d3\u7269\u6807\u51c6\u53c2\u8003\u7269\u8d28\u6750\u6599\u6765\u6e90\uff1a<\/strong>\u8840\u6d46\u53d6\u81ea\u7f8e\u56fd\u5404\u5730\u7684\u5404\u4e2a\u8840\u5e93\uff1a\u5317\u5361\u7f57\u6765\u7eb3\u5dde\u7684\u5a01\u5c14\u660e\u987f\u548c\u683c\u6797\u7ef4\u5c14\uff1b\u4f5b\u7f57\u91cc\u8fbe\u5dde\u6770\u514b\u900a\u7ef4\u5c14\u548c\u5965\u5170\u591a\uff1b\u963f\u62c9\u65af\u52a0\u5dde\u743c\u65af\u535a\u7f57\uff1b\u4e9a\u5229\u6851\u90a3\u5dde\u5f17\u62c9\u683c\u65af\u5854\u592b\uff1b\u76d6\u6d1b\u666e\u548c\u963f\u5c14\u4f2f\u514b\u57fa\uff0c\u65b0\u58a8\u897f\u54e5\u5dde\uff1b\u7530\u7eb3\u897f\u5dde\u5b5f\u83f2\u65af\uff1b\u7f05\u56e0\u5dde\u6ce2\u7279\u5170\u5e02\uff1b\u548c\u4f0a\u5229\u8bfa\u4f0a\u5dde\u5361\u672c\u4ee3\u5c14\u3002<\/p>\n<p><strong>\u4eba\u8840\u6e05\u4e2d\u7684\u591a\u6c2f\u8054\u82ef\uff08PCB\uff09\u540c\u7cfb\u7269\u3001\u6c2f\u5316\u519c\u836f\u548c\u591a\u6eb4\u4e8c\u82ef\u919a\uff08PBDE\uff09\u540c\u7cfb\u7269\u6807\u51c6\u7269\u8d28\u6750\u6599\u7684\u5236\u5907\uff1a<\/strong>\u8840\u6e05\u7684\u5236\u5907\u7531Aalto Scientific\uff0c\u6709\u9650\u516c\u53f8\uff0cCarlsbad\uff0cCA\u8fdb\u884c\u3002\u5728\u7ea4\u7ef4\u86cb\u767d\u6c89\u6dc0\u548c\u8fc7\u6ee4\u540e\uff0c\u5c06\u8840\u6e05\u5408\u5e76\uff08\u603b\u5171\u7ea6200 L\uff09\u5e76\u50a8\u5b58\u57284\u00b0C\u4e0b\u3002\u4e3a\u4e86\u751f\u4ea71957\u5e74\u548c1958\u5e74\u7684SRM\uff0c\u8be5\u6c34\u6c60\u88ab\u4e00\u5206\u4e3a\u4e8c\u3002\u4f7f\u7528\u6821\u51c6\u7684\u81ea\u52a8\u79fb\u6db2\u7ba1\uff0c\u5c0610.7 mL\u7b49\u5206\u8840\u6e05\u5206\u914d\u523030 mL\u7425\u73c0\u8272\u73bb\u7483\u74f6\u4e2d\u3002\u6837\u54c1\u88ab\u51bb\u5e72\uff0c\u5e76\u4e14\u5f53\u8fbe\u5230\u7a33\u5b9a\u7684\u771f\u7a7a\u5ea6\u548c\u6e29\u5ea6\u65f6\u88ab\u8ba4\u4e3a\u662f\u5e72\u71e5\u7684\u3002<\/p>\n<p><strong>\u51bb\u5e72\u975e\u5f3a\u5316\u4eba\u4f53\u8840\u6e05\u4e2d\u7684\u6709\u673a\u6c61\u67d3\u7269\u6807\u51c6\u54c1\u4f7f\u7528\u7684\u5206\u6790\u65b9\u6cd5<\/strong><\/p>\n<p>\u5bf9\u4e8eNIST\u65b9\u6cd51\uff0c\u901a\u8fc7\u6dfb\u52a010.7mL\uff08\u8d28\u91cf\u5df2\u77e5\uff09HPLC\u7ea7\u6c34\uff0c\u5bf910\u4e2a\u5c0f\u74f6\u4e2d\u7684\u6bcf\u4e2a\u5c0f\u74f6\u4e2d\u7684\u51bb\u5e72\u8840\u6e05\u8fdb\u884c\u91cd\u6784\u3002\u5c06\u5df2\u77e5\u91cf\u7684\u5185\u6807\u6eb6\u6db2\uff08\u5305\u542b\u9009\u5b9a\u768413C-\u6807\u8bb0\u7684PCB\u540c\u6e90\u7269\u3001\u9009\u5b9a\u768413C\u6807\u8bb0\u7684\u6740\u866b\u5242\u300113C-\u6807\u8bb0\u591a\u6eb4\u4e8c\u82ef\u919a209\u3001\u6c1f\u5316\u591a\u6eb4\u4e8c\u8054\u82ef\u919a47\u3001PCB 103\u548cPCB 198\uff09\u6dfb\u52a0\u5230\u6bcf\u4e2a\u5c0f\u74f6\u4e2d\uff0c\u5c06\u5176\u8d85\u58f0\u5904\u740615\u5206\u949f\uff0c\u5e76\u4f7f\u5176\u5728\u51b7\u85cf\u4e0b\u5e73\u8861\u8fc7\u591c\u3002\u5c06\u6837\u54c1\u4ece\u51b0\u7bb1\u4e2d\u53d6\u51fa\u5e76\u4f7f\u5176\u8fbe\u5230\u73af\u5883\u6e29\u5ea6\u540e\uff0c\u52a0\u516510mL\u7532\u9178\u4f5c\u4e3a\u53d8\u6027\u5242\uff0c\u7136\u540e\u7acb\u5373\u52a0\u516510mL\u6b63\u5df1\u70f7\u548c\u7532\u57fa\u76841:1\uff08\u4f53\u79ef\u5206\u6570\uff09\u6df7\u5408\u7269C\u79bb\u5fc3\u4ee5\u83b7\u5f97\u5c16\u9510\u7684\u76f8\u8fb9\u754c\uff0c\u5c06\u4e0a\u5c42\u6709\u673a\u76f8\u8f6c\u79fb\u5230\u6d53\u7f29\u5bb9\u5668\u4e2d\u3002\u6bcf\u6b21\u752810mL\u6b63\u5df1\u70f7\u91cd\u590d\u63d0\u53d6\u4e24\u6b21\u3002\u4f7f\u7528\u81ea\u52a8\u84b8\u53d1\u7cfb\u7edf\u5c06\u5408\u5e76\u7684\u5df1\u70f7\u5c42\u6d53\u7f29\u81f3\u7ea64 mL\u3002\u5c06\u7ea62 mL\u6d53\u786b\u9178\u52a0\u5165\u5230\u5177\u6709\u65cb\u6d41\u7684\u6d53\u7f29\u5bb9\u5668\u4e2d\u3002\u76f8\u5206\u79bb\u540e\uff0c\u9664\u53bb\u5df1\u70f7\u76f8\uff0c\u5e76\u4f7f\u75284mL\u4efd\u7684\u6b63\u5df1\u70f7\u6d17\u6da4\u786b\u9178\u76f8\u4e24\u6b21\u3002\u5c06\u5408\u5e76\u7684\u5df1\u70f7\u76f8\u6d53\u7f29\u81f3\u7ea60.5mL\uff0c\u7528\u4e8e\u4e8c\u6c27\u5316\u7845\u56fa\u76f8\u8403\u53d6\uff08SPE\uff09\u51c0\u5316\u3002\u752815mL\u5728\u5df1\u70f7\u4e2d\u768410%\uff08\u4f53\u79ef\u5206\u6570\uff09\u4e8c\u6c2f\u7532\u70f7\u6d17\u8131\u611f\u5174\u8da3\u7684\u7ea7\u5206\u3002\u4f7f\u7528\u5728\u7535\u5b50\u51b2\u51fb\uff08EI\uff09\u548c\u8d1f\u79bb\u5b50\u5316\u5b66\u7535\u79bb\uff08NICI\uff09\u6a21\u5f0f\u4e0b\u64cd\u4f5c\u7684\u6c14\u76f8\u8272\u8c31\/\u8d28\u8c31\uff08GC\/MS\uff09\u5bf9\u6d53\u7f29\u6837\u54c1\u8fdb\u884c\u5206\u6790\u3002\u542b\u6709\u975e\u6781\u6027\u4e13\u6709\u76f8\uff08DB-XLB\uff0c\u5b89\u6377\u4f26\u6280\u672f\u516c\u53f8\uff0c\u5fb7\u56fd\u5a01\u5c14\u660e\u987f\uff090.25\u00b5m\u819c\u539a\u76840.25 mm\u00d760 m\u7194\u878d\u4e8c\u6c27\u5316\u7845\u6bdb\u7ec6\u7ba1\u67f1\u7528\u4e8eEI\u5206\u6790\uff08NIST\u65b9\u6cd51a\uff09\uff0c\u800c\u542b\u670950%\uff08\u6469\u5c14\u5206\u6570\uff09\u82ef\u57fa\u53d6\u4ee3\u7684\u7532\u57fa\u805a\u7845\u6c27\u70f7\u76f8\uff08DB-17MS\uff0c\u5b89\u6377\u4f26\u7279\u6280\u672f\u516c\u53f8\uff09\u76840.25 mm\uff1f0 m\u7194\u878d\u4e8c\u6c27\u5316\u7845\u6bdb\u7ec6\u67f1\u7528\u4e8eNICI\u5206\u6790\uff08NIST\u6cd51b\uff09\u3002\u6240\u6709\u6ce8\u5c04\u5747\u4e3a1\u00b5L\uff0c\u4f7f\u7528\u67f1\u4e0a\u5165\u53e3\u3002<\/p>\n<p>\u5bf9\u4e8eNIST\u65b9\u6cd52\uff0c\u901a\u8fc7\u6dfb\u52a010.7mL\uff08\u8d28\u91cf\u5df2\u77e5\uff09HPLC\u7ea7\u6c34\uff0c\u5bf9\u516d\u4e2a\u5c0f\u74f6\u4e2d\u7684\u6bcf\u4e2a\u5c0f\u74f6\u4e2d\u7684\u51bb\u5e72\u8840\u6e05\u8fdb\u884c\u91cd\u6784\u3002\u5c06\u5df2\u77e5\u91cf\u7684\u5185\u6807\u6eb6\u6db2\uff08\u5305\u542b\u9009\u5b9a\u768413C-\u6807\u8bb0\u7684\u591a\u6c2f\u8054\u82ef\u540c\u7cfb\u7269\u3001\u9009\u5b9a\u768413C\u6807\u8bb0\u7684\u519c\u836f\u300113C-\u6807\u8bb0\u591a\u6eb4\u4e8c\u82ef\u919a209\u548c\u9009\u5b9a\u7684\u6c1f\u5316\u591a\u6eb4\u4e8c\u8054\u82ef\u540c\u7cfb\u7269\uff09\u6dfb\u52a0\u5230\u6765\u81ea\u6bcf\u4e2a\u5c0f\u74f6\u76842g\u8840\u6e05\u5b50\u6837\u54c1\u4e2d\uff0c\u6da1\u65cb\uff0c\u5e76\u5728\u51b7\u85cf\u4e0b\u5e73\u8861\u8fc7\u591c\u3002\u5c06\u6837\u54c1\u4ece\u51b0\u7bb1\u4e2d\u53d6\u51fa\u5e76\u4f7f\u5176\u8fbe\u5230\u73af\u5883\u6e29\u5ea6\u540e\uff0c\u52a0\u51652mL\u7532\u9178\uff0c\u7136\u540e\u52a0\u51653mL\u5728\u5df1\u70f7\u4e2d\u768420%\uff08\u4f53\u79ef\u5206\u6570\uff09\u4e8c\u6c2f\u7532\u70f7\u3002\u4f7f\u7528\u805a\u7126\u5fae\u6ce2\u63d0\u53d6\u6cd5\u63d0\u53d6\u6837\u54c1\u3002\u63d0\u53d6\u540e\uff0c\u79bb\u5fc3\u6837\u54c1\uff0c\u9664\u53bb\u6709\u673a\u76f8\uff0c\u518d\u52a0\u51653mL\u768420%\uff08\u4f53\u79ef\u5206\u6570\uff09\u4e8c\u6c2f\u7532\u70f7\u7684\u5df1\u70f7\u6eb6\u6db2\u3002\u91cd\u590d\u63d0\u53d6\uff0c\u5e76\u5408\u5e76\u6709\u673a\u76f8\u3002\u5728\u7528\u6eb6\u5242\u4ea4\u6362\u4e3a\u5f02\u8f9b\u70f7\u8fdb\u884c\u6d53\u7f29\u540e\uff0c\u5728\u786b\u9178-\u4e8c\u6c27\u5316\u7845\u67f1\u4e0a\u6e05\u6d17\u6837\u54c1\uff0c\u7136\u540e\u5728\u6c27\u5316\u94dd\u67f1\u4e0a\u6e05\u6d17\uff085%\u5931\u6d3b\uff09\u3002\u5c06\u6765\u81ea\u51c0\u5316\u67f1\u7684\u6d17\u8131\u6db2\u6d53\u7f29\u81f30.2mL\uff0c\u5c06\u6eb6\u5242\u6539\u4e3a\u5f02\u8f9b\u70f7\u8fdb\u884c\u5206\u6790\u3002\u4f7f\u7528GC\/MS\u5728EI\u6a21\u5f0f\uff08NIST\u65b9\u6cd52a\uff09\u4e0b\u5206\u6790\u6d53\u7f29\u6837\u54c1\uff0c\u4f7f\u75280.18mm\u00d730m\u7684\u7194\u878d\u4e8c\u6c27\u5316\u7845\u6bdb\u7ec6\u7ba1\u67f1\uff0c\u8be5\u6bdb\u7ec6\u7ba1\u67f1\u542b\u67095%\uff08\u6469\u5c14\u5206\u6570\uff09\u82ef\u57fa\u53d6\u4ee3\u7684\u7532\u57fa\u805a\u7845\u6c27\u70f7\u76f8\uff08DB-5MS\uff0c\u5b89\u6377\u4f26\u6280\u672f\u516c\u53f8\uff090.18\u00b5m\u7684\u819c\u539a\u3002\u6240\u6709\u6ce8\u5c04\u5747\u4e3a20\u00b5L\uff0c\u4f7f\u7528\u53ef\u7f16\u7a0b\u6e29\u5ea6\u84b8\u53d1\uff08PTV\uff09\u5165\u53e3\u3002\u5bf9\u4e8eNIST\u65b9\u6cd52b\uff0c\u76f8\u540c\u7684\u63d0\u53d6\u7269\u3001\u76f8\u540c\u7684\u67f1\u548cPTV\u5165\u53e3\u4e0eNICI\u6a21\u5f0f\u4e0b\u7684GC\/MS\u4e00\u8d77\u4f7f\u7528\u3002\u5bf9\u4e8eNIST\u65b9\u6cd52c\uff0c\u901a\u8fc7GC\/MS\u5728NICI\u6a21\u5f0f\u4e0b\u5206\u6790\u76f8\u540c\u7684\u63d0\u53d6\u7269\uff0c\u4f7f\u7528\u67f1\u4e0a\u6ce8\u5c04\u5230\u542b\u67095%\uff08\u6469\u5c14\u5206\u6570\uff09\u82ef\u57fa\u53d6\u4ee3\u7684\u7532\u57fa\u805a\u7845\u6c27\u70f7\u76f8\uff08DB-5MS\uff0cAgilent Technologies\uff09\u76840.18 mm\u00d710 m\u7194\u878d\u4e8c\u6c27\u5316\u7845\u6bdb\u7ec6\u7ba1\u67f1\u4e2d\uff0c\u819c\u539a0.18\u00b5m\u3002<\/p>\n<p>\u5bf9\u4e8eNIST\u65b9\u6cd53\uff0c\u901a\u8fc7\u6dfb\u52a010.7mL\uff08\u8d28\u91cf\u5df2\u77e5\uff09HPLC\u7ea7\u6c34\uff0c\u5bf9\u516d\u4e2a\u74f6\u5b50\u4e2d\u7684\u6bcf\u4e2a\u74f6\u5b50\u4e2d\u7684\u51bb\u5e72\u8840\u6e05\u8fdb\u884c\u91cd\u6784\u3002\u5c06\u5df2\u77e5\u91cf\u7684\u5185\u6807\u6eb6\u6db2\uff08\u542b\u6709\u9009\u5b9a\u768413C-\u6807\u8bb0\u7684\u7f9f\u57fa\u5316\u5316\u5408\u7269\uff09\u52a0\u5165\u5230\u6bcf\u4e2a\u5c0f\u74f6\u4e2d\uff0c\u6da1\u65cb\uff0c\u5e76\u5728\u51b7\u85cf\u4e0b\u5e73\u8861\u8fc7\u591c\u3002\u5c06\u6837\u54c1\u4ece\u51b0\u7bb1\u4e2d\u53d6\u51fa\u5e76\u4f7f\u5176\u8fbe\u5230\u73af\u5883\u6e29\u5ea6\u540e\uff0c\u5411\u8840\u6e05\u6837\u54c1\u4e2d\u52a0\u51652mL\u7532\u9178\u548c0.5mL 6mol\/L\u76d0\u9178\uff08HCl\uff09\uff0c\u7136\u540e\u52a0\u51652mL 20%\uff08\u4f53\u79ef\u5206\u6570\uff09\u4e8c\u6c2f\u7532\u70f7\u7684\u5df1\u70f7\u6eb6\u6db2\u3002\u4f7f\u7528\u805a\u7126\u5fae\u6ce2\u63d0\u53d6\u6cd5\u63d0\u53d6\u6837\u54c1\u3002\u5728\u63d0\u53d6\u8fc7\u7a0b\u4e2d\uff0c\u79bb\u5fc3\u6837\u54c1\uff0c\u53bb\u9664\u6709\u673a\u76f8\uff0c\u518d\u52a0\u51653 mL 20%\uff08\u4f53\u79ef\u5206\u6570\uff09\u4e8c\u6c2f\u7532\u70f7\u7684\u5df1\u70f7\u6eb6\u6db2\u3002\u91cd\u590d\u63d0\u53d6\uff0c\u5e76\u5408\u5e76\u6709\u673a\u76f8\u3002\u7136\u540e\u5c06\u6c22\u6c27\u5316\u94be\uff08KOH\uff09\u52a0\u5165\u5230\u6709\u673a\u76f8\u4e2d\u3002\u5c06\u6837\u54c1\u632f\u8361\u63d0\u53d615\u5206\u949f\u5e76\u79bb\u5fc3\uff0c\u5e76\u53bb\u9664KOH\u3002\u8be5\u6b65\u9aa4\u91cd\u590d\u4e24\u6b21\uff0cKOH\u76f8\u5408\u5e76\u3002\u5c06HCl\uff086mol\/L\uff09\u52a0\u5165\u5230KOH\u76f8\u4e2d\uff0c\u968f\u540e\u52a0\u51652mL 20%\uff08\u4f53\u79ef\u5206\u6570\uff09\u4e8c\u6c2f\u7532\u70f7\u7684\u5df1\u70f7\u6eb6\u6db2\u3002\u9664\u53bb\u5df1\u70f7\u76f8\uff0c\u5e76\u5c06\u8be5\u6b65\u9aa4\u91cd\u590d\u4e24\u6b21\uff0c\u5408\u5e76\u5df1\u70f7\u76f8\u3002\u4f7f\u7528\u7845\u80f6\u67f1\u8fdb\u884c\u51c0\u5316\uff0c\u7136\u540e\u4f7f\u7528\u6db2\u76f8\u8272\u8c31\u6cd5\u548c\u4e09\u91cd\u56db\u6781\u8d28\u8c31\u4eea\uff08LC\/MS\/MS\uff09\u8fdb\u884c\u5206\u6790\uff0c\u4f7f\u7528C18\u67f1\uff08Agilent Eclipse Plus C18\uff0c3.0 mm\u00d7150 mm\u00d73.5\u03bcm\uff0cAgilent Technologies\uff09\u548c\u7532\u9187-\u6c34\u68af\u5ea6\u3002<\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u672c\u6807\u51c6\u53c2\u8003\u7269\u8d28\uff08SRM\uff09\u7528\u4e8e\u8bc4\u4f30\u6d4b\u5b9a\u4eba\u4f53\u8840\u6e05\u548c\u7c7b\u4f3c\u57fa\u8d28\u4e2d\u9009\u5b9a\u7684\u591a\u6c2f\u8054\u82ef\uff08PCB\uff09\u540c\u7cfb\u7269\u3001\u6c2f\u5316\u519c\u836f\u548c\u591a\u6eb4\u4e8c\u82ef\u919a\uff08PBDE\uff09\u540c\u7cfb\u7269\u7684\u5206\u6790\u65b9\u6cd5\u3002\u63d0\u4f9b\u4e86\u9009\u5b9a\u7684\u591a\u6c2f\u4e8c\u82ef\u5e76\u5bf9\u4e8c\u6076\u82f1\uff08PCDDs\uff09\u3001\u591a\u6c2f\u4e8c\u5e76\u544b\u5583\uff08PCDFs\uff09\u3001\u5168\u6c1f\u5316\u5408\u7269\uff08PFCs\uff09\u548c\u8840\u8102\u7684\u53c2\u8003\u503c\u3002\u63d0\u4f9b\u4e86\u6240\u9009\u7f9f\u57fa\u5316\u5316\u5408\u7269\u7684\u4fe1\u606f\u503c\u3002SRM 1957\u4e2d\u63d0\u4f9b\u4e86\u5176\u503c\u7684\u6240\u6709\u6210\u5206\u90fd\u5929\u7136\u5b58\u5728\u4e8e\u51b7\u51bb\u5e72\u71e5\u7684\u4eba\u8840\u6e05\u4e2d\u3002SRM 1957\u7684\u4e00\u4e2a\u5355\u5143\u7531\u4e94\u4e2a30\u6beb\u5347\u7684\u5c0f\u74f6\u7ec4\u6210\uff0c\u6bcf\u4e2a\u5c0f\u74f6\u542b\u6709\u51b7\u51bb\u5e72\u71e5\u7684\u975e\u5f3a\u5316\u4eba\u7c7b\u8840\u6e05\u3002\u4f7f\u7528\u524d\uff0c\u6bcf\u4e2a\u5c0f\u74f6\u4e2d\u7684\u8840\u6e05\u5fc5\u987b\u752810.7 mL\u84b8\u998f\u6c34\u6216HPLC\u7ea7\u6c34\u91cd\u65b0\u914d\u5236\u3002SRM 1957\u7684\u5f00\u53d1\u662f\u7f8e\u56fd\u56fd\u5bb6\u6807\u51c6\u4e0e\u6280\u672f\u7814\u7a76\u6240\uff08NIST\uff09\u4e0e\u7f8e\u56fd\u75be\u75c5\u63a7\u5236\u4e0e\u9884\u9632\u4e2d\u5fc3\uff08CDC\uff09\u6709\u673a\u5206\u6790\u6bd2\u7406\u5b66\u5904\u5b9e\u9a8c\u5ba4\u79d1\u5b66\u90e8\u7684\u5408\u4f5c\u3002<\/p>\n","protected":false},"featured_media":85697,"comment_status":"closed","ping_status":"closed","template":"","meta":{"site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"default","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","theme-transparent-header-meta":"default","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"set","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"ast-content-background-meta":{"desktop":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}}},"product_cat":[25,24,21,91,81,23],"product_tag":[],"_links":{"self":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/product\/104259"}],"collection":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/product"}],"about":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/types\/product"}],"replies":[{"embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/comments?post=104259"}],"wp:featuredmedia":[{"embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/media\/85697"}],"wp:attachment":[{"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/media?parent=104259"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/product_cat?post=104259"},{"taxonomy":"product_tag","embeddable":true,"href":"http:\/\/www.broadbio.com\/wp-json\/wp\/v2\/product_tag?post=104259"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}